Volume 10 Issue 1 ( March 2023 )

Pages_139-145

Synthesis of WO3/Pt Nanoparticle by Microwave-assisted Sol-gel Method for Enhanced Photocatalytic Property in Visible Light

Hendri Widiyandari, Yahya Ayash, Muhammad Shalahuddin Al Ja’farawy, Agus Subagio, Wahyu Bambang Widayatno

[ABSTRACT ]

Pt co-catalyst WO3 (WO3/Pt) nanoparticle has been synthesized with a variation of platinum co-catalyst mass percentage using the microwave-assisted sol-gel method. The XRD characterization results show that WO3/Pt has a triclinic (anorthic) crystal structure. The touch diagram from UV-Vis DRS measurement exhibits that the energy band gap value of pristine WO3 nanoparticle of 2.89 eV, while for WO3/Pt was in the range of 3.23 – 3.43 eV. PL spectra depicted the photoluminescence intensity decreasing by the addition of Pt. WO3/Pt improved photocatalytic properties in the degradation of methylene blue (MB) under visible light for 30 min irradiation up to 98.7% degraded.

Keywords: tungsten oxide; platinum; nanoparticle; microwave assisted sol-gel; photocatalyst