The Effects of Piper nigrum Soaking Temperature, Density, and Sacking on its Stiffness Measured Using our Tailor Made Pepper Stiffness Instrument
1Research Center for Photonics, BRIN, Indonesia
2Department of Physics, IPB University, Indonesia
3Research Center for Testing Technology and Standards, BRIN, Indonesia
*Author to whom correspondence should be addressed:
E-mail: sens001@brin.go.id (SW)
E-mail: sens001@brin.go.id (SW)
Received: June 16, 2025 | Revised: April 15, 2026 | Accepted: April 24, 2026 | Published: June 2026
Abstract
This study aims to measure the effects of Piper nigrum soaking temperature, density, and sacking on its stiffness using our tailor-made Piper nigrum stiffness instrument. The soaking water temperature is classified as low (room water temperature), moderate (60 °C), and high temperature (90 °C). The Piper nigrum density is grouped into low (90 gr/2 l), moderate (90 gr/1.5 l), and high density (90 gr/1 l). The Piper nigrum is divided into sacking and non-sacking. The experiment is conducted in three batches. Hence, the total samples are 54 (3 x 3 x 2 x 3). The first batch (18 samples) is divided into three temperature groups, three density groups, and two sacking groups. The second and third samples of temperature groups are treated further with moderate or high temperatures, respectively, for five minutes. The first batch is lifted from the soaking tubs for natural drying. These processes are repeated for the second and third batches. The stiffness measurements, from 11352.56 N/m to 20356.32 N/m, were obtained. The results tested using three-way Anova with a 5 % (0.05) significance level (95 % confidence level) showed that there were significant interactions among Piper nigrum soaking temperature, density, and sacking on its stiffness.
Keywords
density; Piper nigrum pericarp stiffness; Piper nigrum stiffness instrument; sacking; soaking temperature
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- 1) D. Rustandi, Irmansyah, S. Wijonarko, M. Kurniati and T. Maftukhah, "The role of thermal and electrical energies to increase the pepper quality: A review," in IOP Conf. Series: Earth and Environmental Science 1344, Bali, 2024
- 2) D. Rustandi, Irmansyah, M. Kurniati, S. Wijonarko, S. W. Hidayat, T. Maftukhah and Mahmudi, "A control system for pepper submersion tub actuators," in Journal of Physiscs: Conference Serries, 2973 012009, Belitung, 2025 doi:10.1088/1742-6596/2973/1/012009
- 3) G. Wu, C. Zhang, X. Li, Z. Niu, X. Jiang, J. Zhang, L. You, J. Li, Y. Liu, Y. Liu, H. Wu and W. Hu, "Purification and characterization of a novel peroxidase from pepper (Piper nigrum L.)," LWT - Food Sci. Technol.,, vol. 214, pp. 1-10, 2024 doi:10.1016/j.lwt.2024.117149
- 4) S. A. Purnamasari and D. Setyaningsih, "The drying temperature impact on curcumin - piperine dissolution and its kinetic release: Application of a spray dryer on the preparation of solid dispersion-based microparticle containing curcuma longa and Piper nigrum extracts," J. Res. Pharm.,, vol. 27, no. 4, p. 1329-1337 (2023) doi:10.29228/jrp.420
- 5) J. P. M. OliveiraI, G. O. EvertonI and V. E. M. Filho, "Green synthesis and biotechnological profile of silver nanoparticles using Piper nigrum L. essential oil," Ciência e Nat., vol. v, no. 46, pp. 1-19, 2024 doi:10.5902/2179460X74388
- 6) M. Khajeh, M. Ghaffari-Moghaddam, A. B. J. Piri, H. Senol and D. Saloglu, "Using microwave-assisted extraction with advanced artificial intelligence models for predicting tannins in black pepper (Piper nigrum L.)," J. Appl. Res. Med. Aromat. Plant, vol. 44, p. 1-8 (2025). 2025 doi:10.1016/j.jarmap.2024.100594
- 7) R. Varghese and J. G. Ray, "Ecology of endomycorrhizal association in black pepper (Piper nigrum L.), South India," J. Appl. Res. Med. Aromat. Plants, vol. 45, pp. 1-20, 2025 doi:10.1016/j.jarmap.2024.100617
- 8) E. Sampepana, A. Rinaldi, T. Nurwidayati and S. H. Saputra, "Moisture content, piperine and essential oils of pepper produced by SME Samboja, SME Bontang and those circulated in Samarinda market," JRTI, vol. 42, pp. 275-283, 2020 doi:10.26578/jrti.v1
- 9) BSN, SNI 01- 0005-1995 Lada Hitam, Jakarta: BSN, 1995
- 10) BSN, SNI 0004:2013 Lada Putih, Jakarta:: BSN, 2013
- 11) S. M. Somashekar, K. K. Subraya, S. K. Vijayan and S. B. Pillai, "Pericarp as a new berry trait to define dry recovery and quality in black pepper (Piper nigrum L.)," Sci. Hortic. (Amsterdam), vol. 281, pp. 1-7, 1099, 2021 doi:10.1016/j.scienta.2021
- 12) J. T. Sulhatun, "Pemanfaatan lada hitam sebagai bahan baku pembuatan oleoresin dengan metode ekstraksi," J. Teknol. Kim. Unimal, vol. 22, p. 16-30, 2013
- 13) N. S. Aziz, N. S. S. Seng, N. S. M. Razali, S. J. Lim and W. A. W. Mustapha, "A review on conventional and biotechnological approaches in white pepper production," Sci Food Agric,, vol. 99, no. 6, pp. 2665-2676, 2019 doi:10.1002/jsfa.9481
- 14) R. W. Arief, D. R. Mustikawati and R. Asnawi, "Karakteristik mutu lada hitam dan lada putih dari beberapa kabupaten sentra lada di Lampung," in Seminar Nasional dalam Rangka Dies Natalis ke-44 UNS Tahun 2020 Strategi Ketahanan Pangan Masa New Normal Covid-19, pp. 111-116, 2022
- 15) Y. Fu, S. C. X. Wang, L. Wang, Z. Wang, Y. Cheng, Y. Liu, L. Zhang, S. Liu, J. Kang and C. Li, "Insights into the correlation between microbial community succession and pericarp degradation during pepper (Piper nigrum L.) peeling process via retting," Foods, vol. 12, pp. 1-14, 2024 doi:10.3390/foods13111615
- 16) E. Karmawati, I. K. Ardana, Siswanto and D. Soetopo, "Factors effecting pepper production and quality in several production center," in IOP Conference Series: Earth and Environmental Science, 1-10, 012051, 2020 doi:10.1088/1755-1315/418/1/
- 17) P. N. M. A. Azman, R. Shamsudin, H. C. Man and M. E. Ya’acob, "Effects of flowing water on soaking water quality during the retting process of pepper berries (Piper Nigrum L.)," Adv. Agric. Food Res. J.,, vol. 3, no.1, p. 1-10. 2022 doi:10.36877/aafrj.a
- 18) Kamila, R. Kusmiadi and N. S. Aini, "Impact aisessment of immersion time delaying and threshing on quality of Muntok white pepper," J. Bioind., vol. 01, no. 02, p. 213-228, 2019
- 19) Hernani, T. Hidayat and E. Sukasih, "Processing of white pepper through the combination of soaking and boiling time towards the quality," Int. J. Technol., vol. 14, no. 5, pp. 1147-1156, 2023 doi:10.14716/ijtech.v14i5.4169
- 20) V. Vinod, A. Kumar and T. J. Zachariah, "Isolation, characterization and identification of pericarp-degrading bacteria for the production of off-odour-free white pepper from fresh berries of Piper nigrum L.," J. Appl. Microbiol., vol. 116, pp. 890--902, 2014 doi:10.1111/jam.12431
- 21) R. Kusmiadi, S. N. Aini and Nurkholis, "Analysis of mature and physiological aspects of soaking method physical and chemical white pepper (Muntok White Pepper)," Agrosainstek, vol. 1, no. 1, p. 39-48, 2017
- 22) P. N. M. A. Azman, R. Shamsudin, H. C. Man and M. E. Ya’acob, "Kinetics of quality changes in soaking water during the retting process of pepper berries (Piper nigrum L.)," Processes, vol. 8, pp. 1-11, 2020 doi:10.3390/pr8101255
- 23) Y. Huang, X. Wang, Y. Lyu, Y. Li, R. He and H. Chen, "Metabolomics analysis reveals the non-enzymatic browning mechanism of green peppers (Piper nigrum L.) during the hot-air drying process," Food Chem., vol. 464, pp. 1-14, 2025 doi:10.1016/j.foodchem
- 24) M. H. Hamzah, A. S. Amran, A. F. A. Hamzah, M. Z. M. Nor, R. Shamsudin, H. C. Man and W. A. W. Razali, "Durian waste husks as an adsorbent in improving soaking water during the retting process of Piper nigrum L. (Pepper Berries)," Separations, vol. 10, no. 96, pp. 1-15, 2023 doi:10.3390/separations10020096
- 25) S. Desai, V. S. Sharanagat and P. K. Nema, "Dielectric Roasting Induced Physical, Mechanical, and Grinding Characteristics of Black Pepper (Piper nigrum)," J. Food Process. Preserv., vol. 1, pp. 1-12, 2023 doi:10.1155/2023/9052417
- 26) S. Gutt, G. Gutt, T.-L. Severin, S. Mironeasa, M. Poroch-Seritan and F.-C. Alexuc, "Equipment for material testing and advanced characterization," in Intelligent Manufacturing & Automation: Power Of Knowledge And Creativity, 697-698, 2011
- 27) S. Gutt, G. Gutt, T.-L. Severin, M. Poroch-Seritan, S. Mironeasa and M. A. Oroian, "Portable hardness tester," in Proceedings of the 22nd International DAAAM Symposium, B. Katalinic, Ed., Vienna: DAAAM International, 0699-0700, 2011
- 28) G. Gutt, S. Gutt, M. Poroch-Seritan, T.-L. Severin and S.-G. Stroke, "Contribution regarding the achievement of portable hardness tester and it’s applications," Metal, vol. 20, no. 5, p. 1-17, 2011
- 29) A. Vaško, J. Sovík and M. Krynke, "Determination of accuracy and reliability of portable hardness testers," Qual. Prod. Improv., vol. 1, no. 1, pp. 289-295, 2019 doi:10.2478/9783110680591-039
- 30) F. R. Harker, R. L. Amos, G. Echeverría and F. A. Gunson, "Influence of texture on taste: Insights gained during studies of hardness, juiciness, and sweetness of apple fruit," J. Food Sci., vol. 71, no. 2, p. S77–S82, 2006
- 31) S. K. R. Shreelavaniya, "Effect of moisture content on physical properties of black pepper," Int.J.Curr.Microbiol.App.Sci,, vol. 6, no. 10, pp. 4873-4879, 2017.610.456, 2017 doi:10.20546/ijcmas
- 32) W. S. Q. L. C. L. J. L. S. Li, "Assessing fruit hardness in robot hands using electric gripper actuators with tactile sensors," Sensors Actuators A. Phys., vol. 365, pp. 1-10, 2024 doi:10.1016/j.sna.2023.114843
- 33) Z. Zhang, J. Zhou, Z. Yan, K. Wang, J. Mao and Z. Jiang, "Hardness recognition of fruits and vegetables based on tactile array information of manipulator," Comput. Electron. Agric., vol. 181, pp. 1-10, 2021 doi:10.1016/j.compag.2020.105959
- 34) J. A. Prakosa, P. Purwowibowo, E. Kurniawan, S. Wijonarko, T. Maftukhah, D. Rustandi, E. B. Pratiwi and R. Rahmanto, "Experimental design of fast terminal sliding mode control for valve regulation under water load uncertainty for precision irrigation," Actuators, vol. 12, no. 155, pp. 1-13, 10.3390/act12040155, 2023
- 35) E. Kurniawan, J. A. Prakosa, H. Wang, S. Wijonarko, T. Maftukhah, P. Purwowibowo, H. Septanto, E. B. Pratiwi and D. Rustandi, "Design of fractional order odd-harmonics repetitive controller for discrete-time linear systems with experimental validations," Sensors, vol. 22, pp. 1-17, 2022
- 36) B. H. Sirenden, P. Mursanto and S. Wijonarko, "Galois field transformation effect onspace-time-volume velocimetry methodfor water surface velocity video analysis," Multimedia Tools and Applications, pp. 1-22, 10.1007/s11042-022-13627-z, 2022
- 37) S. Wijonarko and T. Maftukhah, "Instrumentation system for water balance measurements on Serkuk subbasin, Kubu watershed, Belitung," in AIP Conference Proceedings, Yogyakarta, 2016
- 38) T. Maftukhah, S. Wijonarko, Purwowibowo, D. Rustandi, Mahmudi, S. W. Hidayat, J. A. Prakosa, E. Kartarajasa and I. M. Siburian, "A method to present the uniqueness for uniform program applied in irrigation telecontrol," Evergreen, vol. 10, no. 03, pp. 1708-1716, 2023
- 39) A. Kumar, A. K. Chanda and S. Angra, "Numerical modelling of a composite sandwich structure having non metallic honeycomb core," Evergreen, vol. 8, no. 4 doi.org/10.5109/4742119,pp. 759-767, 2021
- 40) C. T. Murthy and S. Bhattacharya, "Moisture dependant physical and uniaxial compression properties of black pepper," J. Food Engineeting, vol. 37, p. 193-205, 1998
- 41) P. N. M. A. Azman, R. Shamsudin, H. C. Man and M. E. Ya’acob, "Some physical properties and mass modelling of pepper berries (Piper nigrum L.), variety Kuching, at different maturity levels,"," Processes, vol. 8, pp. 1-15, 10.3390/pr8101314, 2020
- 42) S. Usmiati and N. Nurdjannah, "Pengaruh lama perendaman dan cara pengeringan terhadap mutu lada putih," J. Tek. Ind. Pert., vol. 16, no. 3, p. 91-98, 2007
- 43) L. Yu, X. Hu, R. Xu, Y. Ba, X. Chen, X. Wang, B. Cao and X. Wu, "Amide alkaloids characterization and neuroprotective properties of Piper nigrum L.: A comparative study with fruits, pericarp, stalks and leaves," Food Chem., vol. 368, pp. 1-8, 130832, 2022 doi:10.1016/j.foodchem.2021
- 44) A. N. S. A. Khorairi, N.-S. Sofian-Seng, R. Othaman, N. S. M. Razal and K. F. Kasim, "Assessment of natural cellulosic powder from pepper pericarp waste (Piper nigrum L.) after alkalization and bleaching treatment: Effect of alkali concentration and treatment cycle," Sains Malaysiana, vol. 51, no. 4, pp. 1061-1074, 2022 doi:10.17576/jsm-2022-5104-09
- 45) T. Hidayat, Risfaheri and N. Nurdjannah, "Pengaruh perlakuan buah lada sebelum pengupasan dan kecepatan putaran piringan terhadap kinerja alat pengupas lada yang dimodifikasi," Buletin Penelitian Tanaman Rempah dan Obat, pp. 19-28, 2002
- 46) K. Valenta, H. D. Bhramdat, G. V. Calhoun, D. J. Daegling and O. Nevo, "Variation in ripe fruit hardness: a mechanical constraint?," Oikos, vol. 2022, no. 2, p. 10.1111/ oik.08074
- 47) A. Kumar, A. K. Chanda and S. Angra, "Optimization of Stiffness Properties of Composite Sandwich," Evergreen, vol. 08, no. 02, pp. 310-317, 2021
- 48) S. Wijonarko, D. Rustandi, T. Maftukhah, Purwowibowo, A. Setiono, D. Hanto, H. Pratomo, S. W. Hidayat and Mahmudi, "Metode jatuhan dan alat ukur kekerasan kulit lada sehabis perendaman". Indonesia Patent Patent P00202410229, 2024
- 49) N. Z. A. Bakar and M. H. Padzillah, "Comparison between computational fluid dynamics and fluid-structure interaction models of an automotive mixed flow turbocharger turbine," Evergreen, vol. 11, no. 02, pp. 1457-1470, 2024
- 50) Ganta, M. Gezahagn and M. Patel, "Evaluation of mechanical and thermal properties of alkali-treated sisal, bamboo, and hybrid fiber-reinforced polymer composites," Evergreen, vol. 11, no. 3, pp. 1784-1797, 2024
- 51) W. Navidi, Statistics for Engineers and Scientists, New York:: McGraw-Hill Education, 2020
- 52) V. Ordonez, H. Baykara, A. Riofrio, M. Cornejo and R. Rodríguez, "Preparation and characterization of ecuadorian bamboo fiber-low-density polyethylene (LDPE) biocomposites," Evergreen, vol. 10, no. 01, pp. 43-54, 2023
- 53) H. Sosiati, Hidayatullah and S. Hamdan, "Effect of woven e-glass and bamboo stacking sequences on the properties of laminated composites using polyester matrix filled with eggshell microparticles," Evergreen, pp. 693-700, 2024
- 54) D. Ariawan, W. P. Raharjo, K. Diharjo, W. W. Raharjo and B. Kusharjanta, "Influence of water immersion on flexural and impact strength of microcrystalline cellulose- added unsaturated polyester-matriced composites strengthened by untreated, fumigated and alkalized cantala fibers," Evergreen, vol. 11, no. 03, pp. 2164-2174, 2024
- 55) M. G. Ganta and P. Mahaboob, "Evaluation of mechanical and thermal properties of alkali treated sisal, bamboo, and hybrid fiber-reinforced polymer composites," Evergreen, vol. 11, no. 03, pp. 1784-1797, 2024
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